Intergranular Corrosion Test (IGC) per ASTM A At TCR Engineering Services, several methods exist for the testing of intergranular corrosion. To conduct. Detecting Susceptibility to Intergranular Attack in Austenitic Stainless Steels. ASTM A is the specification which governs five practices used to determine if the. Abstract. A detailed study of AISI and stainless steels (SSs) has been conducted to correlate the degree of sensitization (DOS) measured by the.
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Share on Tumblr Print. This abstract is a brief summary of the referenced standard. ISO is specifically for duplex and all austenitic stainless steels, and recommends ageing at two different temperatures: It depends on which Practice is selected, but typically ranges from to days for different tests.
ASTM G28 method B is a more aggressive test than method A and is intended for more corrosion resistant alloys, aetm listed in the document.
ASTM A Intergranular Corrosion Testing and Analysis
In many cases we can reduce that to as little as 24 hours more than the required testing time if you need fast results. ASTM G28 does not require samples to be heat treated.
It does not say what to do about duplex or super austenitic alloys. Our knowledgeable scientists have the experience and expertise necessary to determine the most appropriate intergranular attack testing methods for your material while providing actionable results you can rely on.
The ASTM A tests can determine if the proper heat treatment was performed or if the alloys are in danger of intergranular corrosion occurring in use. Similar to the Streicher test, the Huey test method uses a nitric acid solution and subjects the specimen to five hour boiling intervals. The Copper Sulfate Test is especially effective for determining susceptibility to intergranular attack for low carbon steels. What is your typical turnaround time? SEP also gives guidance on which of its methods apply to which alloys: The test is generally performed for acceptance of materials, but not sufficient for rejection of materials.
None of these are identical and cross substitution of results is not possible. The latter is a German test, but it is often called up in European projects. Table 1 below shows the various methods for four common standards: There are other requirements in these standards over details that are not discussed in this document, and these should be followed, such as conducting bend tests. Strauss test specimens are boiled in a Copper Sulfate – Sulfuric Acid mixture for 15 hours.
Alternatively, a welded test-piece in the as-welded condition may be tested. Choosing the correct method s rely on a complete understanding of your material and processes, as well as the concept of corrosion itself. ISO is the most rigorous in terms of defining test methods, and says which alloys should use which test methods as follows: Since high temperature processing such as heat treatment is a common practice, many manufacturers wish to perform intergranular corrosion qualification testing on each batch, to ensure that the material has been processed correctly and does not show signs of corrosion susceptibility.
Link to Active This link will always route to the current Active version of the standard. The chart below comes from the ASTM A standard for selection of the appropriate test by alloy type:.
We provide intergranular corrosion evaluation, salt spray testing, stress corrosion, and various other methods to simulate exposure of your products or materials to corrosive environments. Practice A, the oxalic acid etch test is used as a rapid technique to screen samples of certain stainless steel grades to ensure they are not susceptible to intergranular attack sensitization.
For an alloy that is satm listed, look for an alloy with a similar composition to a listed alloy to determine the most suitable test. The exception to this is ASTM G28 method A, where rates for the onset of intergranular corrosion are described in reference 1.
It has been used for the duplex stainless steel UNS Sasrm has been used for nitric acid cooler tubes. This practice includes boiling the sample for 24 to hours in the solution above, and measures the materials performance quantitatively. For many alloys, the onset is at 0. If the structure is acceptable no additional testing is required. Typical examination magnification is X to X.
Please specify the maximum allowable corrosion rate and any available data on the sensitizing heat treatment performed. It can be seen that some alloys fall into two categories, and no guidelines are given for selecting the most appropriate. ASTM G28 lists alloys and specifies the test exposure for each. ASTM A testing is a popular method of choice due to the variety of practices available and the relatively short turnaround for results.
Choosing an Intergranular Corrosion Test Method Since high temperature processing such as heat treatment is a common practice, many manufacturers wish to perform intergranular corrosion qualification testing on each batch, to ensure that the material has been processed correctly and does not show signs of corrosion susceptibility.
Get in Touch Contact us by Phone or Email to find out how we can help your industry. Hence, it is normally only used for stainless steels intended for nuclear service, or another application involving nitric acid. Where a bend test is required, the sample must be bent over a mandrel of a diameter related to the specimen diameter, without any cracking, as determined by inspection under a low power microscope and a microsection in any suspicious areas.
Based on your materials, application, and requirements, the other 4 methods provide specific focuses. If materials with incorrect heat treatment enter service, they are liable to crack or fail by intergranular corrosion IGC much more rapidly than properly treated materials; ASTM A is a screening test to help find batches that are incorrectly processed.
Intergranular Corrosion Tests for CRAs
All five methods within this specification involve exposing specimens to a chemical mixture designed to encourage corrosive behavior. The oxalic acid test is commonly used before the Strauss test to determine if a sample is susceptible; samples that pass method A will generally show low corrosion rates in the Strauss test.
In everyday applications, corrosion varies by materials and solutions. A different ASTM A test method must be used to quantify the level of corrosion or to disqualify a material for a2262. This method is a hour boiling test for a62 received” specimens of stainless steel.
These practices include five intergranular corrosion tests, namely: Contact us now for pricing or a quote! It is informational only and not an official part of the standard; the full text of the standard itself must be referred to for its use and application.
The Huey test works well to analyze chromium depleted regions and intermetallic precipitates, such as a62 phase, and is also used for materials in strongly oxidizing environments asstm as nitric acid. The test evaluates the resistance of extra-low-carbon steels to sensitization and intergranular attack from welding or heat treatment processes.